Synthesis of Terpinene-maleic Anhydride Adduct Catalyzed by the Solid Super Acid SO 4 2- /TiO 2 CatalystChinese Full Text
YU Shitao,SONG Zhanqian Research Institute of Chemical Processing and Utilization of Forest Products,CAF,Nanjing,China 210042.
Abstract: The solid super acid SO 4 2- /TiO 2 was first used in catalytic synthesis of terpinene-maleic anhydride adduct(TMA).The suitable conditions of preparation of the catalyst and synthesis of TMA were obtained:concentration of H 2SO 4=0.10~0.25mol/L,calcination temperature=500~550℃,calcination time=3h and the amount of catalyst=10% of maleic anhydride,molar ratio of maleic anhydride to turpentine=1/1.8~1/2.2,reaction temperature=130~150℃,reaction time=2.5~3.0h.The relation between activity a... More
Keywords:
- Series:
(B) Chemistry/ Metallurgy/ Environment/ Mine Industry
- Subject:
Organic Chemical Industry
- Classification Code:
TQ436.94
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